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Electron Guns have been used since the late 1940s in [https://en.wikipedia.org/wiki/Cathode-ray_tube  cathode ray tube] (CRT) televisions and monitors. <br />
Electron guns have been used since the late 1940s in [https://en.wikipedia.org/wiki/Cathode-ray_tube  cathode ray tube] (CRT) televisions and monitors.


The design of our electron gun can be understood through its two separate functions: electron emission and electron acceleration. Namely, to first introduce electrons into the system and then to accelerate these electrons, in a controlled manner, towards a target.
The design of our electron gun project can be understood through its two separate functions: electron emission and electron acceleration. In summary, to introduce electrons into the system and then to accelerate these electrons in a controlled manner towards a target.


The introduction of electrons is done through thermionic emission. An electric current is passed through a filament which will then undergo Joule Heating. Thermionic emission will take place once the filament is sufficiently heated. This introduces electrons into the system.   
The introduction of electrons is done through thermionic emission. An electric current is passed through a filament which will undergo Joule heating. Thermionic emission will take place once the filament is sufficiently heated, hence introducing the electrons into the system.   


The acceleration is achieved by differentially biasing electrodes within the electron gun to create an electric field that will accelerate the electrons towards the target in a controlled manner. The last clause requires more than mere potential differences but electrostatic lenses such that the electron beam can be coaxed into a desired trajectory. Broadly, both these objectives are achieved by having an acceleration section followed by a focusing section. 
The acceleration of electrons is achieved by differentially biasing electrodes within the electron gun to create an electric field that will accelerate the electrons towards the target in a controlled manner. The last clause requires more than mere potential differences but electrostatic lenses such that the electron beam can be coaxed into a desired trajectory.


Directly following Thermionic emission, the electrons are subject to an accelerating potential. This accelerating potential is provided by an electrode (termed the anode) which is held at a positive potential difference from the filament. This causes electrons emitted from the filament to be accelerated towards the plate. Working in tandem with the anode is the Wenhelt Cylinder. Once accelerated past the anode, the beam is focused, again, with an Einzel lens.  
Broadly, both these objectives would be achieved by having an acceleration section, followed by a focusing section.


These two, loosely defined, steps should result in an electron beam that is focused on a target. The target could be anything from a screen coated in phosphorous (to show the beam spot) to a Faraday Cup which can then be connected to a current measurement device.
Directly following thermionic emission, the electrons are subject to an accelerating potential. This accelerating potential is provided by an electrode (anode) which is held at a positive potential difference with respect to the filament. This causes electrons emitted from the filament to be accelerated towards the plate. Working in tandem with the anode is the Wenhelt Cylinder. Once accelerated past the anode, the beam is again once more with an Einzel lens.
 
These two loosely defined steps should result in an electron beam that is focused on a target. The target could be anything from a screen coated in phosphorous (to show the beam spot), to a Faraday Cup which is connected to a current measurement device.


==Team Members==
==Team Members==
Aliki Sofia Rotelli (A0236272H)<br />
The group consists of 4 team members, listed below in alphabetical order.
Lai Tian Hao (A0236351L)<br />
 
Lim En Liang, Irvin (A0173028J)<br />
* Aliki Sofia Rotelli (A0236272H)
Tan Chuan Jie (A0154805E)
* Lai Tian Hao (A0236351L)
* Lim En Liang, Irvin (A0173028J)
* Tan Chuan Jie (A0154805E)


==Idea==
==Idea==
There are two parts to this project. The first would be to create the electron source which seems to be done with the use of a Lenard/Crookes tube [https://en.wikipedia.org/wiki/Crookes_tube]. Secondly, we would want to focus this electron beam into a spot with the use of a homemade magnetic lens (probably a solenoid of some form). We could perhaps perform a measurement of the focal length with respect to the magnetic field strength of the lens.
The project is divided into two parts.
 
===Electron source===
An electron source would be fabricated with the use of a [https://en.wikipedia.org/wiki/Crookes_tube Lenard/Crookes tube]. This tube is an electrical experimental discharge tube within a vacuum system that generates electrons by ionisation of the remaining air molecules within the chamber. The project would hence be built in a vacuum chamber.
 
===Collimated beam===
The generated electrons would need to be collimated into a beam with the use of a homemade magnetic lens (a solenoid of some form). To observe this beam, a material capable of showing the electron spot would hence be needed in our project.


==Concepts==
==Concepts==
===Focusing Lens===
===Focusing Lens===
====Beam Resolution====
====Beam Resolution====
One of the most important considerations scaling down is the Rayleigh criteria. The Rayleigh criteria relates the critical dimension (CD), or smallest feasible feature size resolvable by an optical system, to the imaging wavelength (𝜆) and numerical aperture (NA). This criteria is crucial. As a result of decreasing the critical dimension.
One of the most important considerations in the scaling down portion is the [https://en.wikipedia.org/wiki/Angular_resolution#The_Rayleigh_criterion Rayleigh Criterion]. The Rayleigh Criterion relates the critical dimension (CD), or smallest feasible feature size resolvable by an optical system, to the imaging wavelength (<math>\lambda</math>) and numerical aperture (NA). This criteria is crucial as a result of a small CD, as shown in the equations below.


<math> Critical Dimension =  \frac{(0.61)\lambda}{(NA = n_1 Sin(\theta_1))} </math> <br />
<math>NA = n sin(\theta)</math>


====The Wehnelt cylinder====
<math>CD =  0.61\frac{\lambda}{NA} </math>
The Wehnhelt cylinder is a negatively biased cylinder located right after the filament. It influences the focusing of the electron beam and the electron emission from the filament. When tuned appropriately, the Wenhelt Cylinder, together with the anode, aids in the emission of electrons from the filament by creating a net electric field from the attractive (to the electrons) anode and repulsive Wehnelt. Being negatively biased, the Wehnelt cylinder also acts as a convergent electrostatic lens which focuses the electron beam path from the filament to the anode.
 
In the above equations, ''θ'' is the maximum half-angle of the light cone that enters or exits the lens, ''n'' is the [https://en.wikipedia.org/wiki/Refractive_index refractive index] of the medium, ''λ'' is the wavelength of light.
 
====Wehnelt Cylinder====
The Wehnelt cylinder is a negatively biased cylinder located right after the electron source. It affects the focusing of the electron beam and the electron emission from the source. When tuned appropriately, the Wehnelt cylinder, together with the anode, aids in the emission of electrons from the source by creating a net electric field from the attractive anode and repulsive Wehnelt cylinder. Being negatively biased, the Wehnelt cylinder also acts as a convergent electrostatic lens which focuses the electron beam path from the filament to the anode.


====Einzel Lens====
====Einzel Lens====
Like the Wehnelt Cylinder, the Einzel lens is also an electrostatic lens. In this electron gun, the Einzel lens is made of three cylindrical tubes in series along the direction of the electron beam. Due to the electrostatic symmetry, the ions do not lose energy through the focusing process. In operation only the middle Einzel is actively biased (positively). The other components of the lens being held at ground potential.
Similar to the Wehnelt cylinder, the Einzel lens is also an electrostatic lens. In this project, the Einzel lens would be made of three cylindrical tubes in series along the direction of the electron beam.
 
Due to the electrostatic symmetry, the ions do not lose energy through the focusing process. In operation, only the middle Einzel lens is actively biased (positively). The other components of the lens are held at ground potential.


====Schematic of Electron gun====
====Schematic of Electron gun====


[[File:SchematicEgun.png|700px|thumb|none|Schematic of Electron gun]]
[[File:SchematicEgun.png|thumb|none|640px|Schematic of Electron gun]]
 
The electrical schematic is concerned with controlling the potentials of critical components. These components are the Wenhelt cylinder, Anode, and Einzel lens. A separate distinction would be the polarity of these components. Both the Anode and Einzel lens would be positively biased up to 1 kV above ground while the Wenhelt Cylinder will be negatively biased down to 1 kV below ground (i.e. -1 kV). These values are simply ranges and specific potential values were determined through simulations. The components would be biased to recreate the conditions in the simulations.
 
Each of these potentials would be achieved with separate high voltage Power Supply Units (PSUs). Due to the shortage of devices, only 2 PSUs were used. This was achieved by biasing both the Anode and Einzel lens to the same potentials, thus allowing one PSU to be used for both. The simulations suggested that this configuration would provide sufficient acceleration and focusing effects on the electron beam.
 
The actual practical set-up is more accurately depicted in the schematics below.
 
[[File:Practical Electrical Setup.jpeg|thumb|none|640px|Updated practical schematic of Electron gun for operation with only two High Voltage Power Supplies]]


====Simulated Proof of Concept====
====Simulated Proof of Concept====
Simulations were performed in SIMION based on a proposed arrangement of the components mentioned above. <br />
Simulations were performed in a simulation software, SIMION, based on the above-mentioned proposed configuration.
With parameters: <br />
 
*Wehnelt: -200V <br />
{| class="wikitable"
*Anode: 1000V  <br />
|+ Simulation Parameters
*Middle Einzel: 500V <br />
|-
| Wehnelt || -200 V
|-
| Anode || 1000 V
|-
| Middle Einzel || 500 V
|}
 
[[File:A Simulation of ebeam.jpeg|thumb|none|640px|A Simulation of the focused electron beam with Wehnelt cylinder and Einzel lens (Top-Down Cross-Sectional View)]]
[[File:Simulationisoview.png|thumb|none|360px|A Simulation of the focused electron beam with Wehnelt cylinder and Einzel lens (Isometric View)]]
[[File:Simulationpotentials.png|thumb|none|360px|A Simulation of the focused electron beam with Wehnelt cylinder and Einzel lens (Potential Field)]]
 
The above shows an ideal situation. However, in practical set-ups, the space is constrained and all the items had to be placed closer to each other. This results in the set-ups depicted below, with all simulations at top-down cross-sectional view.
 
[[File:Compact EGun Einzel 0V.jpeg|thumb|none|640px|Revised simulation at 0 V]]
[[File:Compact EGun Einzel 200V.jpeg|thumb|none|640px|Revised simulation at 200 V]]
[[File:Compact EGun Einzel 400V.jpeg|thumb|none|640px|Revised simulation at 400 V]]
[[File:Compact EGun Einzel 600V.jpeg|thumb|none|640px|Revised simulation at 600 V]]
[[File:Compact EGun Einzel 800V.jpeg|thumb|none|640px|Revised simulation at 800 V]]
[[File:Compact EGun Einzel 900V.jpeg|thumb|none|640px|Revised simulation at 900 V]]
[[File:Compact EGun Einzel 1kV.jpeg|thumb|none|640px|Revised simulation at 1000 V]]
 
As shown, even with the compacting of the electron gun, a focused beam spot is still able to be produced with the following parameters.


<div><ul>
{| class="wikitable"
<li style="display: inline-block;"> [[File:A Simulation of ebeam.jpeg|thumb|none|715px|A Simulation of the focused electron beam with Wehnelt cylinder and Einzel lens (Top-Down Cross-Sectional View)]] </li>
|+ Simulation Parameters
<li style="display: inline-block;"> [[File:Simulationisoview.png|thumb|none|350px|A Simulation of the focused electron beam with Wehnelt cylinder and Einzel lens (Isometric View)]] </li>
! Item !! Original !! Revised
<li style="display: inline-block;"> [[File:Simulationpotentials.png|thumb|none|350px|A Simulation of the focused electron beam with Wehnelt cylinder and Einzel lens (Potential Field)]] </li>
|-
</ul></div>
| Wehnelt || -200 V || -200 V
|-
| Anode || 1000 V || 1000 V
|-
| Middle Einzel || 500 V || 900-1000 V
|}


===Design of the electron gun's "central column"===
===Design of the electron gun's "central column"===
Based on the schematic of the simulation, the development of a "central column" was designed using SOLIDWORKS, which consists of
Based on the schematic of the simulation, the development of a "central column" was designed using a 3D Computer-Aided Design (CAD) software, SOLIDWORKS. It consists of 4 main components as described below.
*Acrylic plate
*Einzel lens
*Anode
*Wehnelt cylinder


====Acrylic Plate====
====Acrylic Plate====
The acrylic plate was created in a disk shape with a 100mm outside diameter and a 28mm inner diameter. In addition, the disk's inner ring features a 1mm by 32mm (depth/diameter) recessed on both sides. The recessed was created to allow for the secure installation of subsequent elements.<br />
[[File:Acylic plate.png|360px|thumb|none|Schematic design of Acylic plates]]
<br />
 
[[File:Acylic plate.png|400px|thumb|none|Schematic design of Acylic plates]]
The acrylic plate was created in a disk shape with a 100 mm outer diameter and a 28 mm inner diameter. In addition, the disk's inner ring features a 1 mm depth with 32 mm diameter recessed on both sides. The recess was created to allow for the secure installation of subsequent elements.
 
====Einzel Lens====
[[File:Einzel lens.png|360px|thumb|none|Schematic design of Einzel lens]]


====Einzel lens====
The three components of the Einzel was designed with dimensions:
The three components of the Einzel was designed with dimensions:
*Outer diameter: 32mm
*Outer diameter: 32 mm
*Inner diameter: 28mm
*Inner diameter: 28 mm
*Length: 30mm
*Length: 30 mm


[[File:Einzel lens.png|400px|thumb|none|Schematic design of Einzel lens]]
====Anode====
[[File:Anode.png|360px|thumb|none|Schematic design of Anode]]


====Anode====
The anode was designed with dimensions:
The anode was designed with dimensions:
*Outer diameter: 32mm
*Outer diameter: 32 mm
*Apeture (diameter): 8mm
*Aperture (diameter): 8 mm
*Thickness: 2mm
*Thickness: 2 mm
 
[[File:Anode.png|400px|thumb|none|Schematic design of Anode]]


====Wehnelt cylinder====
====Wehnelt Cylinder====
*Outer diameter: 32mm
[[File:Wehnelt cylinder.png|360px|thumb|none|Schematic design of Wehnelt cylinder]]
*Inner diameter: 28mm
*Apeture (diameter): 8mm
*Length: 30mm


[[File:Wehnelt cylinder.png|400px|thumb|none|Schematic design of Wehnelt cylinder]]
The Wehnelt cylinder was designed with dimensions:
*Outer diameter: 32 mm
*Inner diameter: 28 mm
*Aperture (diameter): 8 mm
*Length: 30 mm


===="Central column" design====
===="Central Column" design====
[[File:Schematic design inner.png|700px|thumb|none|Central Column Schematic Design of Electron Gun]]
[[File:Schematic design inner.png|640px|thumb|none|Central Column Schematic Design of Electron Gun]]


====Central column with chamber design====
===="Central Column" with Chamber design====
[[File:Schematic diagram overview.png|700px|thumb|none|Schematic diagram overview of electron gun]]
[[File:Schematic diagram overview.png|640px|thumb|none|Schematic diagram overview of electron gun]]


==Equipment & Components==
==Equipment & Components==
The following items were considered for the system:
To build the electron gun, the following items were considered for the system.


===High Vacuum (HV) Components===
===High Vacuum (HV) Components===
* Roughing Pump
* Roughing Pump (RP)
* Turbo-Molecular Pump
* Turbo-Molecular Pump (TMP)


===Electrical Components===
===Electrical Components===
* High Voltage Power Supply Unit (PSU) (up to 5kV)
* 2 x PHYWE High voltage power supply with digital display (10 kV DC, 2 mA)
* Current Controlled PSU
* Current Controlled PSU


Line 108: Line 156:
===Measurement Components===
===Measurement Components===
* High Vacuum Digital Gauge, with range <math>(10^{-3}</math> ~ <math>10^{-7})</math> mbars
* High Vacuum Digital Gauge, with range <math>(10^{-3}</math> ~ <math>10^{-7})</math> mbars
**Edwards PRM10 (Pirani Gauge)
** Edwards PRM10 ([https://en.wikipedia.org/wiki/Pirani_gauge Pirani Gauge])
**Edwards D145-41-000 (Penning Gauge)
** Edwards D145-41-000 ([https://en.wikipedia.org/wiki/Pressure_measurement#Cold_cathode Penning Gauge])


===Other Components===
===Other Components===
Line 120: Line 168:
* CF-40 Copper Gaskets
* CF-40 Copper Gaskets


==Setup==
==Main Set-Up==
===Manufacturing of central column===
===Central Column===
All of the items listed below were made in the workshop.
All of the items listed below were made in the CQT workshop located in S15 level 1.
 
====Acrylic Plate====
====Acrylic Plate====
The laser cutter is unable to make cuts at varying heights. To work around the laser cutter's limitations, a different approach was devised. First, a disk was cut out of a 5mm thick acrylic sheet with an outer radius of 100mm and an inner diameter of 32mm. Second, a 32mm/28mm (outer/inner) diameter ring was cut. Following that, the pieces were put together with an adhesive compound that allowed for a 1mm recess on both sides of the disk.<br />
The laser cutter was unable to make cuts at varying heights. To work around this limitation, a different approach was devised.
<br />
 
[Insert photo of acrylic plate]<br />
First, a disk was cut out of a 5 mm thick acrylic sheet with an outer radius of 100 mm and an inner diameter of 32 mm. Next, a 32 mm/28 mm (outer/inner) diameter ring was cut. Finally, the pieces were put together with an adhesive compound that allowed for a 1 mm recess on both sides of the disk.
<br />
 
Nine additional disks were manufactured in the same manner to obtain a total of ten disk plates.
9 additional disks were manufactured in the same manner to obtain a total of 10 disk plates.
<br />
 
====Einzel Lens, Anode, Wehnelt Cylinder====
[[File:Lathe drilling.gif|360px|thumb|none|A drill bit with a diameter of 28mm was used to remove aluminum rod material with a lathe (GIF)]]
 
The Einzel lens, Anode, and Wehnelt cylinders were sculpted out from a single aluminum rod with a length of 350 mm and a diameter of 42 mm. A lathe (a machine that rotates a workpiece about an axis of rotation to perform an operation such as cutting, sanding, drilling, etc.) was used for the fabrication of these 3 components.
 
Upon clamping down the aluminum rod securely, the rotational gears were set to "low" with a rotational speed of 105 and 610 rounds per minute (RPM), with a large and small drill bit respectively. The drill bit was secured within the "tail stock".
 
[[File:Facing of einzel lens.gif|500px|thumb|none|Rotational gear: low-610 RPM, Removal of the surface material of aluminum rod ("Facing") (GIF)]]


====Lathe Machine: Drilling====
After achieving the structure's inner diameter, a "facing" tool was used to remove the surface material from the outside construction, "thinning" it from 42 mm to 32 mm. Rotational gear speed was set to 610 RPM when "facing".
The three components of the Einzel lens, anode, and Wehnelt cylinder were sculpted out from a 42mm by 350mm (diameter/length) aluminum rod with the use of a lathe (a machine that rotates a workpiece about an axis of rotation to perform an operation such as cutting, sanding, drilling, etc.). After securely clamping down the aluminum rod, the rotational gears were set to “low” with a rotational speed of 105/610 rounds per minute (RPM) based on drill bit size: (Large/Small), and a drill bit secured within the “Tail Stock”.  
<br />


[[File:Lathe drilling.gif|500px|thumb|none|A drill bit with a diameter of 28mm was used to remove aluminum rod material with a lathe (GIF).]]
====Electron Source====
The electron source, a filament, was also prepared by breaking a bulb. The glass was broken by lightly tapping the bulb with a metal hammer in a plastic bag. Broken glass fragments were then cleaned up.


====Lathe Machine: "Facing"====
====Photos====
After achieving the structure's inner diameter, a "facing" tool was used to remove the surface material from the outside construction, "thinning" it from 42mm to 32mm. Rotational gear was set to low-610 RPM when "facing."
The 3 components and the filament were successfully prepared for the system.
<br />


[[File:Facing of einzel lens.gif|500px|thumb|none|Rotational gear: low-610 RPM, Removal of the surface material of aluminum rod ("Facing") (GIF).]]
[[File:Wehnelt manufactured.jpeg|thumb|none|360px|Manufactured Wehnelt Cylinder]]
[[File:Manufactured Anode.jpeg|thumb|none|360px|Manufactured Anode]]
[[File:Manufactured einzel.jpeg|thumb|none|360px|Manufactured Einzel]]
[[File:Filament.jpeg|360px|thumb|none|Prepared Electron Source (filament)]]


====Manufactured items====
===Chamber Preparation===
The following items were manufactured for the system.  
To prepare the chamber, latex gloves were worn to prevent contamination due to natural oil and minerals on the skin. Any contamination would result in low vacuum performance.
<div><ul>
<li style="display: inline-block;"> [[File:Wehnelt manufactured.jpeg|thumb|none|300px|Manufactured wehnelt cylinder]] </li>
<li style="display: inline-block;"> [[File:Manufactured Anode.jpeg|thumb|none|300px|Manufactured Anode]] </li>
<li style="display: inline-block;"> [[File:Manufactured einzel.jpeg|thumb|none|300px|Manufactured Einzel]] </li>
</ul></div>


Other than the manufactured items mentioned above, the filament was also prepared. The glass of the bulb was broken by lightly tapping the bulb with a metal hammer in a plastic bag. Broken glass fragments are then disposed of, resulting in the following:
====Electron Source====
[[File:Filament assembly.jpeg|300px|thumb|none|Assembly of the first component (electron source)]]


[[File:Filament.jpeg|300px|thumb|none|Broken bulb with exposed filament]]
M5 nuts were utilized as a locking mechanism to ensure that the acrylic plates were firmly secured in place. The nuts were inserted both above and below the plates.


===Chamber Setup===
====Wehnelt Cylinder====
Note: Latex gloves were worn during the setup of the external ports of the chamber and the assembly of the centre column.
[[File:Wehnelt in column.jpeg|thumb|none|360px|Placement of the Wehnelt cylinder within the central column stack]]
[[File:Wehnelt in column 2.jpeg|thumb|none|360px|Placement of the Wehnelt cylinder within the central column stack (side profile)]]


*M5 nuts were utilized as a locking mechanism to guarantee that acrylic plates were firmly secured in place (Top and bottom of the acrylic plates).
The Wehnelt cylinder was carefully lowered into the chamber. Care has been taken to ensure that it does not touch the filament.
[[File:Filament assembly.jpeg|300px|thumb|none|Assembly of first component (Filament).]]


*The wehnelt cylinder was then carefully lowed into the chamber to ensure no contact between it and the filament.
====Other Components====
[[File:Full stack.jpeg|360px|thumb|none|Assembled components including Filament, Wehnelt cylinder, Anode, and Einzel lens]]


<div><ul>
The rest of the components (Anode and 3 Einzel lenses) were assembled fully within the chamber to achieve a full stack that is similar to the illustration of the schematic diagram.
<li style="display: inline-block;"> [[File:Wehnelt in column.jpeg|thumb|none|300px|Placement of the wehnelt cylinder within the central column stack.]] </li>
<li style="display: inline-block;"> [[File:Wehnelt in column 2.jpeg|thumb|none|300px|Placement of the wehnelt cylinder within the central column stack (side profile).]] </li>
</ul></div>


*The rest of the component which includes: the anode and three einzel lens were then assembled within the chamber to achieve a full stack similar to the illustration of the schematic diagram.
====Phosphor Screen====
[[File:Full stack.jpeg|300px|thumb|none|Assembled components which includes: filament, wehnelt cylinder, anode and einzel lens.]]
[[File:Phosphor with kapton.jpeg|thumb|none|360px|Phosphor mounted with Kapton tape (bottom side)]]
[[File:Phosphor with kapton top.jpeg|thumb|none|360px|Phosphor mounted on with Kapton tape (top side)]]


*With the central column setup completed, the phosphor was then mounted on the chamber lid with the use of Kapton tape. (Note: During the process of mounting, glass slide shattered causing a slight misalignment of the phosphor with respect to the center of the column.)
With the central column completed, the phosphor (spread on a 1" by 2" cover slide) was mounted on the chamber lid with the use of Kapton tape.


<div><ul>
During the process of mounting, the cover slide shattered, causing a slight misalignment of the phosphor with respect to the center of the column.
<li style="display: inline-block;"> [[File:Phosphor with kapton.jpeg|thumb|none|300px|Phosphor on a microscope glass mounted on with Kapton tape (bottom side).]] </li>
<li style="display: inline-block;"> [[File:Phosphor with kapton top.jpeg|thumb|none|300px|Phosphor on a microscope glass mounted on with Kapton tape (top side).]] </li>
</ul></div>


===Fully Assembled System===
===Fully Assembled System===
[[File:Full setup.jpeg|500px|thumb|none|Fully assembled setup]]
[[File:Full setup.jpeg|640px|thumb|none|Fully assembled set-up]]
 
The system was fully assembled with the RP and TMP installed with a gauge reading the chamber pressure. The PHYWE PSUs were also attached through the external feed-throughs.
 
==Measurements and Tests==
 
===Conductance Test===
A conductance test of individual components were performed during to ensure proper connections between the components and the feedthroughs.
 
[[File:Conductivity test.jpeg|360px|thumb|none|Demonstration of checking for proper connection with a multimeter]]
[[File:Connection.png|thumb|none|360px|Feedthrough connections]]


==Measurements/Test==
===Phosphor Characterization===
===Phosphor Characterization===
The phosphor powder used in this project was kindly provided by Nejilock. The composition is >99% zinc sulfide. We characterized the powder using a fluorescent microscope. The powder is excited with UV light and the emission is collected. The spectrum of wavelengths emitted is presented in the figure below. The majority of the emission is in the 450-550 nm region, meaning the powder will have a blue/green glow.
The phosphor powder used in this project was kindly provided by Nejilock. It has a composition of >99% Zinc Sulfide. The powder can be characterised using a fluorescent microscope.
 
The powder was excited with UV light and the emission was collected. The spectrum of wavelengths emitted is presented in the figure below. The majority of the emission is in the 450-550 nm region, meaning the powder will have a blue/green glow.
 
[[File:Phosphor spectrum.png|360px|thumb|none|The wavelength spectrum of the phosphor]]
 
Several methods to insert the phosphor powder into the system were attempted. The most successful method was to create a paste consisting of a mixture of transparent nail polish. This paste was then added to the powder that was already applied on a small section of the glass slide. Once the thinner evaporates, the powder will be stuck to the glass.
 
===Pressure Characterisation===
The Roughing Pump (RP) and the Turbomolecular Pump (TMP) were both characterised.
 
For a turbo-roughing system, a vacuum pressure of approximately <math>10^{-3}</math> mbar must first be achieved using the RP before the TMP can be turned on, so as to not damage the turbine blades of the TMP.
 
Various pressures at different timings are recorded into the table below.
 
{| class="wikitable"
|+ Chamber pressure
|-
! Time !! Pressure
|-
| 41 min || <math>6.5 \times 10^{-6}</math> mbar
|-
| 16 h|| <math>1.5 \times 10^{-6}</math> mbar
|-
| 48 h|| <math>5.2 \times 10^{-7}</math> mbar
|}
 
The graphs of pressure against time for both RP and TMP were also plotted into logarithmic graphs, as shown below. The RP was transitioned into the TMP at approximately the 1064th second at a pressure of <math>5.2 \times 10^{-3}</math> mbar.
 
[[File:Roughing pump.png|thumb|none|360px|RP pressure graph]]
[[File:Turbo pump.png|thumb|none|360px|TMP pressure graph]]
[[File:Max pressure.jpeg|thumb|none|360px|Vacuum pressure after 48hours of pumping]]
[[File:Turbo.jpeg|thumb|none|360px|Turbo-molecular pump]]
[[File:Roughing2.jpeg|thumb|none|360px|Roughing pump backing the turbo pump]]
 
==Experiment and Results==
 
The experiment was conducted after pumping down the chamber for several hours in a dark environment. Care was taken such that the 1000 V PSU was provided with ample safety precautions.
 
The final parameters were tuned with similar simulation parameters.
 
{| class="wikitable"
|+ Simulation Parameters
|-
| Wehnelt || -200 V
|-
| Anode || 1000 V
|-
| Middle Einzel || 1000 V
|}
 
As mentioned, because of the identical potential for the Anode and Einzel lens, the same power supply was able to be used for both of them while a separate one was used for the Wehnelt cylinder.
 
[[File:HPS.jpeg|360px|thumb|none|Power supply to Wehnelt cylinder at -200 V and 1 kV to anode and Einzel lens]]
 
The filament power supply was set to 10 V DC. Current provided was 0.1104 A as shown on the filament PSU (Keithley 2200 DC Power Supply).
 
[[File:Filament psu.jpeg|360px|thumb|none|Power supply for tungsten filament]]
 
A tinge of fluorescence can be spotted which is illuminated from the phosphor coating with a more prominent glow located at the top right quadrant. This coincides with the slight misalignment of the glass slides during installation.


[[File:Phosphor spectrum.png|500px|thumb|none|The wavelength spectrum of the phosphor, excited by UV source.]]
[[File:Lumonous.jpeg|360px|thumb|none|Phosphor glow due to focused electron beam]]


===Pressure Characterization===
Due to the low intensity of the fluorescence, no useful data could be taken. The discussion is included in the section below.
The roughing pump and the turbomolecular pump were both characterized while they were connected to the chamber. Do note that for a turbo-roughing system, vacuum pressure criteria of approximately <math>10^{-3}</math>mbar must first be achieved using the roughing pump before the turbomolecular pump can be turned on. This is to ensure that the turbines blades of the turbo remain undamaged. Maximum vacuum pressure achieved with this setup is <math>1.5 \times 10^{-6}</math>mbar after 16 hours and <math>5.2 \times 10^{-7}</math>mbar after 48hours of pump down. With an initial maximum of <math>6.5 \times 10^{-6}</math>mbar at 41mins.


<div><ul>
==Problems and Discussions==
<li style="display: inline-block;"> [[File:Roughing pump.png|thumb|none|700px|The plot of pressure in mbars as a function of time]] </li>
<li style="display: inline-block;"> [[File:Turbo pump.png|thumb|none|700px|The plot of pressure in mbars as a function of time]] </li>
</ul></div>


Throughout the project, various obstacles were met. Methods to overcome them were attempted but not successful.


<div><ul>
===Dim luminescence of phosphor===
<li style="display: inline-block;"> [[File:Max pressure.jpeg|thumb|none|300px|Vacuum pressure after 48hours of pumping]] </li>
When the set-up was running, the glow of the phosphor was barely observed. This could be attributed to the thickness of the phosphorus and the spot size.
<li style="display: inline-block;"> [[File:Turbo.jpeg|thumb|none|300px|Turbo-molecular pump]] </li>
<li style="display: inline-block;"> [[File:Roughing2.jpeg|thumb|none|535px|Roughing pump backing the turbo pump]] </li>
</ul></div>


===Conductance Test===
As mentioned previously, the spot size of the beam would be a few hundred microns. With such a spot size and a thick phosphorus layer, when the beam hits the bottom of the layer, it would illuminate only slightly at the top layer. The phosphor would thus only appear to slightly "glow" and not allowing us to see the spot as expected. To counter this, a thinner layer of phosphor could be fabricated.
After all of the components were assembled, conductance tests of individual components were performed to ensure proper connections between the components and the feedthroughs.
 
A Faraday Cup was initially planned to be included for current measurement, but due to logistical issues, we could not get the picoammeter (RBD 9103) that was indented for the project on time.
 
Another reason for the low luminescence could be due to a low vacuum. With all components installed, the pressure was relatively higher (<math>~10^{-4}</math> mbar) than what was characterised above. One way to overcome this is to clean all components thoroughly again (sandblasting, chemical cleaning, etc.). Unfortunately, it could not be done on time for the module.
 
===Filament alignment===
As the set-up was built from the bottom-up and due to limitations of the size and the holder, the filament could not be adjusted freely, thereby resulting in possibilities of misaligning the filament.


<div><ul>
After the set-up was complete, it was observed that the filament was biased to one side. This affects the results as the simulation assumes the filament to be at the centre of the Wehnelt cylinder.
<li style="display: inline-block;"> [[File:Conductivity test.jpeg|300px|thumb|none|Demonstration of checking for proper connection with a multimeter]] </li>
<li style="display: inline-block;"> [[File:Connection.png|thumb|none|306px|Feedthrough connections]] </li>
</ul></div>


==Experiment/Results==
A future improvement would be to mount the bulb base on a stage with some degrees of freedom. However, this would likely add some height to the base plate, resulting in a need to compact the system further.
Similar to the parameters simulated:
*The wehnelt cylinder at potential: -200V
*Anode and the first and third Einzel lens at the potential: 1kV


[[File:HPS.jpeg|300px|thumb|none|Power supply to wehnelt cylinder at -200V and 1kV to anode and einzel lens.]]
===High Voltage PSUs===
In the current set-up, only 2 PSUs were used to vary the potential differences of the 3 Einzel lenses and the Wehnelt cylinder. An extra power supply would enable the Einzel lens potential differences to be tuned separately, providing better fine-tuning abilities.


*Filament power supply:
===Logistics===
**Voltage: 10V
The project was originally planned to be located in the Physics Acoustic Room (S13 level 1). However, during the course of designing the chamber, the location was shifted to a lab within the Centre of Ion Beam Applications (CIBA), at S7 level 1 as the tools were more readily available there.
**Current: 0.1104A


[[File:Filament psu.jpeg|300px|thumb|none|Power supply for tungsten filament.]]
The chamber design was revised intensively before the current version was reached. The original design had to be scrapped due to a lack of components.


A tinge of fluorescence can be spotted which is illuminated from the phosphor coating. With a more prominent glow located at the top right quadrant of the phosphor coating. This coincides with the slight misalignment of the glass slides during installation.  
===Future===
As the project has caught the attention of another Professor, it will be continued after PC5209 officially ends for the current semester.


[[File:Lumonous.jpeg|300px|thumb|none|Phosphor glow due to focused electron beam]]
==Conclusion==
The electron beam was observed, but limitations meant that we could not measure the beam spot size nor other parameters.


==Potential Problems==
Further attempts and modifications will be planned such that the electron gun will be working for the purpose of other projects that requires it, such as a compact electron imaging system.

Latest revision as of 16:37, 30 April 2022

Electron guns have been used since the late 1940s in cathode ray tube (CRT) televisions and monitors.

The design of our electron gun project can be understood through its two separate functions: electron emission and electron acceleration. In summary, to introduce electrons into the system and then to accelerate these electrons in a controlled manner towards a target.

The introduction of electrons is done through thermionic emission. An electric current is passed through a filament which will undergo Joule heating. Thermionic emission will take place once the filament is sufficiently heated, hence introducing the electrons into the system.

The acceleration of electrons is achieved by differentially biasing electrodes within the electron gun to create an electric field that will accelerate the electrons towards the target in a controlled manner. The last clause requires more than mere potential differences but electrostatic lenses such that the electron beam can be coaxed into a desired trajectory.

Broadly, both these objectives would be achieved by having an acceleration section, followed by a focusing section.

Directly following thermionic emission, the electrons are subject to an accelerating potential. This accelerating potential is provided by an electrode (anode) which is held at a positive potential difference with respect to the filament. This causes electrons emitted from the filament to be accelerated towards the plate. Working in tandem with the anode is the Wenhelt Cylinder. Once accelerated past the anode, the beam is again once more with an Einzel lens.

These two loosely defined steps should result in an electron beam that is focused on a target. The target could be anything from a screen coated in phosphorous (to show the beam spot), to a Faraday Cup which is connected to a current measurement device.

Team Members

The group consists of 4 team members, listed below in alphabetical order.

  • Aliki Sofia Rotelli (A0236272H)
  • Lai Tian Hao (A0236351L)
  • Lim En Liang, Irvin (A0173028J)
  • Tan Chuan Jie (A0154805E)

Idea

The project is divided into two parts.

Electron source

An electron source would be fabricated with the use of a Lenard/Crookes tube. This tube is an electrical experimental discharge tube within a vacuum system that generates electrons by ionisation of the remaining air molecules within the chamber. The project would hence be built in a vacuum chamber.

Collimated beam

The generated electrons would need to be collimated into a beam with the use of a homemade magnetic lens (a solenoid of some form). To observe this beam, a material capable of showing the electron spot would hence be needed in our project.

Concepts

Focusing Lens

Beam Resolution

One of the most important considerations in the scaling down portion is the Rayleigh Criterion. The Rayleigh Criterion relates the critical dimension (CD), or smallest feasible feature size resolvable by an optical system, to the imaging wavelength () and numerical aperture (NA). This criteria is crucial as a result of a small CD, as shown in the equations below.

In the above equations, θ is the maximum half-angle of the light cone that enters or exits the lens, n is the refractive index of the medium, λ is the wavelength of light.

Wehnelt Cylinder

The Wehnelt cylinder is a negatively biased cylinder located right after the electron source. It affects the focusing of the electron beam and the electron emission from the source. When tuned appropriately, the Wehnelt cylinder, together with the anode, aids in the emission of electrons from the source by creating a net electric field from the attractive anode and repulsive Wehnelt cylinder. Being negatively biased, the Wehnelt cylinder also acts as a convergent electrostatic lens which focuses the electron beam path from the filament to the anode.

Einzel Lens

Similar to the Wehnelt cylinder, the Einzel lens is also an electrostatic lens. In this project, the Einzel lens would be made of three cylindrical tubes in series along the direction of the electron beam.

Due to the electrostatic symmetry, the ions do not lose energy through the focusing process. In operation, only the middle Einzel lens is actively biased (positively). The other components of the lens are held at ground potential.

Schematic of Electron gun

Schematic of Electron gun

The electrical schematic is concerned with controlling the potentials of critical components. These components are the Wenhelt cylinder, Anode, and Einzel lens. A separate distinction would be the polarity of these components. Both the Anode and Einzel lens would be positively biased up to 1 kV above ground while the Wenhelt Cylinder will be negatively biased down to 1 kV below ground (i.e. -1 kV). These values are simply ranges and specific potential values were determined through simulations. The components would be biased to recreate the conditions in the simulations.

Each of these potentials would be achieved with separate high voltage Power Supply Units (PSUs). Due to the shortage of devices, only 2 PSUs were used. This was achieved by biasing both the Anode and Einzel lens to the same potentials, thus allowing one PSU to be used for both. The simulations suggested that this configuration would provide sufficient acceleration and focusing effects on the electron beam.

The actual practical set-up is more accurately depicted in the schematics below.

Updated practical schematic of Electron gun for operation with only two High Voltage Power Supplies

Simulated Proof of Concept

Simulations were performed in a simulation software, SIMION, based on the above-mentioned proposed configuration.

Simulation Parameters
Wehnelt -200 V
Anode 1000 V
Middle Einzel 500 V
A Simulation of the focused electron beam with Wehnelt cylinder and Einzel lens (Top-Down Cross-Sectional View)
A Simulation of the focused electron beam with Wehnelt cylinder and Einzel lens (Isometric View)
A Simulation of the focused electron beam with Wehnelt cylinder and Einzel lens (Potential Field)

The above shows an ideal situation. However, in practical set-ups, the space is constrained and all the items had to be placed closer to each other. This results in the set-ups depicted below, with all simulations at top-down cross-sectional view.

Revised simulation at 0 V
Revised simulation at 200 V
Revised simulation at 400 V
Revised simulation at 600 V
Revised simulation at 800 V
Revised simulation at 900 V
Revised simulation at 1000 V

As shown, even with the compacting of the electron gun, a focused beam spot is still able to be produced with the following parameters.

Simulation Parameters
Item Original Revised
Wehnelt -200 V -200 V
Anode 1000 V 1000 V
Middle Einzel 500 V 900-1000 V

Design of the electron gun's "central column"

Based on the schematic of the simulation, the development of a "central column" was designed using a 3D Computer-Aided Design (CAD) software, SOLIDWORKS. It consists of 4 main components as described below.

Acrylic Plate

Schematic design of Acylic plates

The acrylic plate was created in a disk shape with a 100 mm outer diameter and a 28 mm inner diameter. In addition, the disk's inner ring features a 1 mm depth with 32 mm diameter recessed on both sides. The recess was created to allow for the secure installation of subsequent elements.

Einzel Lens

Schematic design of Einzel lens

The three components of the Einzel was designed with dimensions:

  • Outer diameter: 32 mm
  • Inner diameter: 28 mm
  • Length: 30 mm

Anode

Schematic design of Anode

The anode was designed with dimensions:

  • Outer diameter: 32 mm
  • Aperture (diameter): 8 mm
  • Thickness: 2 mm

Wehnelt Cylinder

Schematic design of Wehnelt cylinder

The Wehnelt cylinder was designed with dimensions:

  • Outer diameter: 32 mm
  • Inner diameter: 28 mm
  • Aperture (diameter): 8 mm
  • Length: 30 mm

"Central Column" design

Central Column Schematic Design of Electron Gun

"Central Column" with Chamber design

Schematic diagram overview of electron gun

Equipment & Components

To build the electron gun, the following items were considered for the system.

High Vacuum (HV) Components

  • Roughing Pump (RP)
  • Turbo-Molecular Pump (TMP)

Electrical Components

  • 2 x PHYWE High voltage power supply with digital display (10 kV DC, 2 mA)
  • Current Controlled PSU

Beam Focusing Components

  • Einzel Lens

Measurement Components

  • High Vacuum Digital Gauge, with range ~ mbars

Other Components

Main Set-Up

Central Column

All of the items listed below were made in the CQT workshop located in S15 level 1.

Acrylic Plate

The laser cutter was unable to make cuts at varying heights. To work around this limitation, a different approach was devised.

First, a disk was cut out of a 5 mm thick acrylic sheet with an outer radius of 100 mm and an inner diameter of 32 mm. Next, a 32 mm/28 mm (outer/inner) diameter ring was cut. Finally, the pieces were put together with an adhesive compound that allowed for a 1 mm recess on both sides of the disk.

9 additional disks were manufactured in the same manner to obtain a total of 10 disk plates.

Einzel Lens, Anode, Wehnelt Cylinder

A drill bit with a diameter of 28mm was used to remove aluminum rod material with a lathe (GIF)

The Einzel lens, Anode, and Wehnelt cylinders were sculpted out from a single aluminum rod with a length of 350 mm and a diameter of 42 mm. A lathe (a machine that rotates a workpiece about an axis of rotation to perform an operation such as cutting, sanding, drilling, etc.) was used for the fabrication of these 3 components.

Upon clamping down the aluminum rod securely, the rotational gears were set to "low" with a rotational speed of 105 and 610 rounds per minute (RPM), with a large and small drill bit respectively. The drill bit was secured within the "tail stock".

Rotational gear: low-610 RPM, Removal of the surface material of aluminum rod ("Facing") (GIF)

After achieving the structure's inner diameter, a "facing" tool was used to remove the surface material from the outside construction, "thinning" it from 42 mm to 32 mm. Rotational gear speed was set to 610 RPM when "facing".

Electron Source

The electron source, a filament, was also prepared by breaking a bulb. The glass was broken by lightly tapping the bulb with a metal hammer in a plastic bag. Broken glass fragments were then cleaned up.

Photos

The 3 components and the filament were successfully prepared for the system.

Manufactured Wehnelt Cylinder
Manufactured Anode
Manufactured Einzel
Prepared Electron Source (filament)

Chamber Preparation

To prepare the chamber, latex gloves were worn to prevent contamination due to natural oil and minerals on the skin. Any contamination would result in low vacuum performance.

Electron Source

Assembly of the first component (electron source)

M5 nuts were utilized as a locking mechanism to ensure that the acrylic plates were firmly secured in place. The nuts were inserted both above and below the plates.

Wehnelt Cylinder

Placement of the Wehnelt cylinder within the central column stack
Placement of the Wehnelt cylinder within the central column stack (side profile)

The Wehnelt cylinder was carefully lowered into the chamber. Care has been taken to ensure that it does not touch the filament.

Other Components

Assembled components including Filament, Wehnelt cylinder, Anode, and Einzel lens

The rest of the components (Anode and 3 Einzel lenses) were assembled fully within the chamber to achieve a full stack that is similar to the illustration of the schematic diagram.

Phosphor Screen

Phosphor mounted with Kapton tape (bottom side)
Phosphor mounted on with Kapton tape (top side)

With the central column completed, the phosphor (spread on a 1" by 2" cover slide) was mounted on the chamber lid with the use of Kapton tape.

During the process of mounting, the cover slide shattered, causing a slight misalignment of the phosphor with respect to the center of the column.

Fully Assembled System

Fully assembled set-up

The system was fully assembled with the RP and TMP installed with a gauge reading the chamber pressure. The PHYWE PSUs were also attached through the external feed-throughs.

Measurements and Tests

Conductance Test

A conductance test of individual components were performed during to ensure proper connections between the components and the feedthroughs.

Demonstration of checking for proper connection with a multimeter
Feedthrough connections

Phosphor Characterization

The phosphor powder used in this project was kindly provided by Nejilock. It has a composition of >99% Zinc Sulfide. The powder can be characterised using a fluorescent microscope.

The powder was excited with UV light and the emission was collected. The spectrum of wavelengths emitted is presented in the figure below. The majority of the emission is in the 450-550 nm region, meaning the powder will have a blue/green glow.

The wavelength spectrum of the phosphor

Several methods to insert the phosphor powder into the system were attempted. The most successful method was to create a paste consisting of a mixture of transparent nail polish. This paste was then added to the powder that was already applied on a small section of the glass slide. Once the thinner evaporates, the powder will be stuck to the glass.

Pressure Characterisation

The Roughing Pump (RP) and the Turbomolecular Pump (TMP) were both characterised.

For a turbo-roughing system, a vacuum pressure of approximately mbar must first be achieved using the RP before the TMP can be turned on, so as to not damage the turbine blades of the TMP.

Various pressures at different timings are recorded into the table below.

Chamber pressure
Time Pressure
41 min mbar
16 h mbar
48 h mbar

The graphs of pressure against time for both RP and TMP were also plotted into logarithmic graphs, as shown below. The RP was transitioned into the TMP at approximately the 1064th second at a pressure of mbar.

RP pressure graph
TMP pressure graph
Vacuum pressure after 48hours of pumping
Turbo-molecular pump
Roughing pump backing the turbo pump

Experiment and Results

The experiment was conducted after pumping down the chamber for several hours in a dark environment. Care was taken such that the 1000 V PSU was provided with ample safety precautions.

The final parameters were tuned with similar simulation parameters.

Simulation Parameters
Wehnelt -200 V
Anode 1000 V
Middle Einzel 1000 V

As mentioned, because of the identical potential for the Anode and Einzel lens, the same power supply was able to be used for both of them while a separate one was used for the Wehnelt cylinder.

Power supply to Wehnelt cylinder at -200 V and 1 kV to anode and Einzel lens

The filament power supply was set to 10 V DC. Current provided was 0.1104 A as shown on the filament PSU (Keithley 2200 DC Power Supply).

Power supply for tungsten filament

A tinge of fluorescence can be spotted which is illuminated from the phosphor coating with a more prominent glow located at the top right quadrant. This coincides with the slight misalignment of the glass slides during installation.

Phosphor glow due to focused electron beam

Due to the low intensity of the fluorescence, no useful data could be taken. The discussion is included in the section below.

Problems and Discussions

Throughout the project, various obstacles were met. Methods to overcome them were attempted but not successful.

Dim luminescence of phosphor

When the set-up was running, the glow of the phosphor was barely observed. This could be attributed to the thickness of the phosphorus and the spot size.

As mentioned previously, the spot size of the beam would be a few hundred microns. With such a spot size and a thick phosphorus layer, when the beam hits the bottom of the layer, it would illuminate only slightly at the top layer. The phosphor would thus only appear to slightly "glow" and not allowing us to see the spot as expected. To counter this, a thinner layer of phosphor could be fabricated.

A Faraday Cup was initially planned to be included for current measurement, but due to logistical issues, we could not get the picoammeter (RBD 9103) that was indented for the project on time.

Another reason for the low luminescence could be due to a low vacuum. With all components installed, the pressure was relatively higher ( mbar) than what was characterised above. One way to overcome this is to clean all components thoroughly again (sandblasting, chemical cleaning, etc.). Unfortunately, it could not be done on time for the module.

Filament alignment

As the set-up was built from the bottom-up and due to limitations of the size and the holder, the filament could not be adjusted freely, thereby resulting in possibilities of misaligning the filament.

After the set-up was complete, it was observed that the filament was biased to one side. This affects the results as the simulation assumes the filament to be at the centre of the Wehnelt cylinder.

A future improvement would be to mount the bulb base on a stage with some degrees of freedom. However, this would likely add some height to the base plate, resulting in a need to compact the system further.

High Voltage PSUs

In the current set-up, only 2 PSUs were used to vary the potential differences of the 3 Einzel lenses and the Wehnelt cylinder. An extra power supply would enable the Einzel lens potential differences to be tuned separately, providing better fine-tuning abilities.

Logistics

The project was originally planned to be located in the Physics Acoustic Room (S13 level 1). However, during the course of designing the chamber, the location was shifted to a lab within the Centre of Ion Beam Applications (CIBA), at S7 level 1 as the tools were more readily available there.

The chamber design was revised intensively before the current version was reached. The original design had to be scrapped due to a lack of components.

Future

As the project has caught the attention of another Professor, it will be continued after PC5209 officially ends for the current semester.

Conclusion

The electron beam was observed, but limitations meant that we could not measure the beam spot size nor other parameters.

Further attempts and modifications will be planned such that the electron gun will be working for the purpose of other projects that requires it, such as a compact electron imaging system.